Contents

Definitions/Acronyms

%D
Percent Difference.
%R
Percent Recovery.
AA
Atomic Absorption Spectrometry.
Accuracy
The degree of agreement of a measured value with the true or expected value of the constituent of concern.
Analyst
The staff member who conducts a laboratory analysis or other measurement.
ANSI
American National Standards Institute.
Approval
Denotes agreement with the total action and acceptance of accountability for that action. Approval normally involves signing the document implementing the action.
AS
Analytical spike.
ASME
American Society of Mechanical Engineers.
ASR
Analytical Services Request form. A form used to document critical technical, quality, and administrative requirements and information related to requested work.
ASTM. 1982
Compilation of ASTM Standard Definitions, 5th Edition. Philadelphia, PA.
Average (mean)
The sum of a series of measurements divided by the number of measurements.
BFB
Bromofluorobenzene.
Bias
A systematic error inherent in a method or caused by some artifact or idiosyncrasy of the measurement system.
BS
Blank Spike.
CCB
Continuing calibration blank.
CCV
Continuing calibration verification analytical standard periodically run to monitor instrument stability over time
CERCLA
Comprehensive Environmental Response, Compensation, and Liability Act.
Certification
Process by which recognition is obtained from an appropriate party that a product meets certain specified requirements (ASTM 1982).
Certificate of test
Documentation attesting to the validity of the test performed.
CF
Calibration factor, typically referred to as the Response Factor (RF).
Client
The person, organization, or program from whom samples originate and to whom laboratory results are reported. This may be internal to the laboratory.
CLP
U.S. Environmental Protection Agency Contract Laboratory Program.
Commercial software
Off-the-shelf computer software that is not modified by the user.
Concurrence
Denotes agreement with the proposed action, limited to the area of responsibility of the person concurring.
CVAA
Cold Vapor Atomic Absorption Spectrometry.
CWA
Clean Water Act.
Daily
Each 24-hour time period or the end of an analytical run for those analyses that extend past a 24-hour time period. Daily requirements do not apply on days the instrument is not in use.
DFTPP
Decafluorotriphenylphosphine.
DLR
Decision level count rate.
DOE
U.S. Department of Energy.
DQA
Data quality assessments.
DQO
Data Quality Objectives.
DQR
Data Quality Requirement.
EICP
Extracted ion current profile.
EQL
Estimated quantitation limit the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions.
ES&H
Environmental Safety and Health.
Expiration date
As applied to chemicals and standard materials, a date after which the material may no longer meet specifications.
FLAA
Flame Atomic Absorption Spectrometry.
GC
Gas Chromatography.
GC/MS
Gas Chromatography/Mass Spectrometry.
GFAA
Graphite Furnace Atomic Absorption Spectrometry.
IC
Ion Chromatography.
ICB
Initial calibration blank.
ICN
Interim Change Notice a form for making an editorial correction or simple change to a procedure that provides for identifying, approving, and issuing the change within a short period of time.
ICP-MS
Inductively Coupled Plasma-Mass Spectrometry.
ICV
Initial calibration verification The process of verifying the adequacy of calibration.
IDL
Instrument detection limit the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero. The IDL typically reflects the sensitivity of the analytical system exclusively.
ISE
Ion Selective Electrode.
LCS
Laboratory control sample a control sample of known composition which is analyzed using the same preparation, reagents, and analytical method employed for the sample.
LLS
Low level standard.
LTC
Laboratory Training Coordination a PNNL organization responsible for maintaining auditable training records and a comprehensive training data base for all PNNL staff training.
M&TE
Measuring and test equipment.
MD
Mean difference.
MDA
Minimum detectable activity level of activity that is practically achievable by a measurement system using a specified counting time.
MDC
Minimum detectable concentration the minimum detectable activity divided by additional experimental factors specific to the sample analyzed.
MDL
Method detection limit the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero. The MDL typically reflects the sensitivity of the preparation and analytical process.
MS
Matrix spike.
MSA
Management system assessments.
MSD
Matrix spike duplicate.
NEI NIST
National Energy Institute National Institute of Standards and Technology.
NEPA
National Environmental Policy Act.
PB
Preparation Blank.
PEA
Performance evaluation assessments.
PEM
Performance evaluation mixture.
PNNL
Battelle, Pacific Northwest National Laboratory, operated for the U.S. Department of Energy by Battelle Memorial Institute under Contract DE AC06 76RLO 1830.
Precision
The degree of agreement of independent measurements of a given sample using repeated application of a process under specified conditions.
QA
Quality Assurance A system of activities whose purpose is to provide the producer or user of a product or service the assurance that is meets defined standards of quality. It consists of two separate but related activities, quality control, and quality assessment.
QC
Quality Control a planned system of activities whose purpose is to provide a measurement tool of the quality of a product or service to help ensure that it meets the needs of users. The aim is to provide quality that is satisfactory, adequate, dependable, and economic.
Quality Assessment
System of activities whose purpose is to provide assurance that quality control activities are done effectively. It involves a continuing evaluation of performance of the production system and the quality of products produced.
RCRA
Resource Conservation and Recovery Act.
Reference Material
A material of definite composition that closely resembles, in chemical and physical nature, the material the analyst expects to deal with.
Result
The final quantity (e.g., amount, concentration) obtained from an analysis and reported to the client.
RIDS
Records Inventory and Disposition Schedule/File Index a form used to identify records maintained by file stations that indicates the authorized retention and disposition instructions for those records and also serves as a file index.
RPD
Relative percent difference a mathematical equation that expresses the precision of duplicates.
RRF
Relative Response Factor.
RSD
Relative standard deviation or coefficient of variation.
Sample Custodian(s)
A staff member who receives/handles samples. Project staff trained to this plan may serve as sample custodian.
SAP
Sampling and Analysis Plan.
Shall, Should, and May
Indicators of requirement, recommendation, or permission.
Shall
indicates a requirement that must always be met.
Should
indicates a recommendation but recognizes that exceptions are possible.
May
indicates permission without a recommendation for or against the action.
Signature
Handwritten signature.
SOW
Statement of Work. A document that describes the scope of work for an activity or project. A technical project plan or equivalent work-authorizing document may be also used.
Standard Deviation
(represented by the variable s) A measure of the distribution of a series of replicate measurements around the average of that series.
Standard Material
A material of known composition, confirmed by the preparer.
SW 846
EPA Test Methods for Evaluating Solid Waste.
TC
Total Carbon.
Technical Procedure
Procedures that describe the technical nature of work performed (e.g., preparative and analytical processes). Technical procedures are qualified prior to use on client samples.
Test Plans
Test plans are used when no procedure currently exists which can adequately meet the client DQRs. Test plans provide documentation of the approach that will be taken. The approach is qualified during the execution of the work (no qualification data already exists).
TIC
Total Inorganic Carbon. Specifically in the case of organic GCMS, TIC denotes Tentatively Identified Compounds.
TOC
Total Organic Carbon.
Tri-Party Agreement
Hanford Federal Facility Agreement and Consent Order.
TSA
Technical system assessments.
USEPA
U.S. Environmental Protection Agency.